Cellulose derivatives : synthesis, structure, and properties / Thomas Heinze, Omar A. El Seoud, Andreas Koschella.
This book summarizes recent progress in cellulose chemistry. The last 10 years have witnessed important developments, because sustainability is a major concern. Biodegradable cellulose derivatives, in particular esters and ethers, are employed on a large scale. The recent developments in cellulose c...
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| Main Authors: | , , |
| Format: | eBook |
| Language: | English |
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Cham, Switzerland :
Springer,
2018.
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| Series: | Springer series on polymer and composite materials.
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| Subjects: |
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| 100 | 1 | |a Heinze, Thomas, |d 1958- |e author. |0 http://id.loc.gov/authorities/names/n98018442 |1 http://isni.org/isni/0000000108787133. | |
| 245 | 1 | 0 | |a Cellulose derivatives : |b synthesis, structure, and properties / |c Thomas Heinze, Omar A. El Seoud, Andreas Koschella. |
| 264 | 1 | |a Cham, Switzerland : |b Springer, |c 2018. | |
| 300 | |a 1 online resource. | ||
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| 490 | 1 | |a Springer series on polymer and composite materials. | |
| 504 | |a Includes bibliographical references. | ||
| 505 | 0 | |a Intro; Preface; Organization of This Book; Acknowledgements; Contents; Abbreviations and Symbols; 1 Production and Characteristics of Cellulose from Different Sources; 1.1 Plant Cellulose; 1.1.1 Cellulose from Conventional Sources; 1.1.1.1 Wood; 1.1.1.2 Cotton Linters; 1.1.2 Cellulose from Alternative Sources: Sisal and Agriculture Residues; 1.2 Bacterial Cellulose; 1.3 Structurally Modified Cellulose; 1.3.1 Microcrystalline Cellulose; 1.3.2 Cellulose Whiskers; 1.3.3 Microfibrillated Cellulose; Annex; References; 2 Structure and Properties of Cellulose and Its Derivatives. | |
| 505 | 8 | |a 2.1 Molecular and Supramolecular Structure of Cellulose2.2 Molar Mass and Its Distribution; 2.2.1 Rheology and Viscometry; 2.2.1.1 Theoretical Background; 2.2.1.2 Practical Aspects; 2.2.1.3 Applications of Viscometry in Cellulose Chemistry; 2.2.2 Size Exclusion Chromatography, SEC; 2.2.2.1 Theoretical Background; 2.2.2.2 Practical Aspects; 2.2.3 Light Scattering (LS); 2.2.3.1 Theoretical Background; 2.2.3.2 Practical Aspects; 2.2.4 Use of Integrated Analytical Techniques; 2.3 Structural Information; 2.3.1 X-ray Diffraction; 2.3.1.1 Theoretical Aspects. | |
| 505 | 8 | |a 2.3.1.2 Probing the Structure and Hydrogen Bonding in Cellulose2.3.2 Infrared and Raman Spectroscopy; 2.3.2.1 Theoretical Background; 2.3.2.2 Practical Aspects; 2.3.3 NMR Spectroscopy; 2.3.3.1 Solid-State NMR of Cellulose; 2.3.3.2 Application of Liquid Phase NMR; 2.3.4 Chromatographic Analysis; 2.3.4.1 HPLC Analysis of Cellulose After Degradation; 2.3.4.2 Analysis of Cellulose Derivatives After Degradation; 2.3.4.3 Chromatographic Techniques Applied After Degradation and Subsequent Derivatization; 2.3.5 Mass Spectroscopy (MS); 2.3.6 Thermal Analysis; 2.3.6.1 Theoretical Background. | |
| 505 | 8 | |a 2.3.6.2 Practical Aspectsâ#x80;#x94;Applications of TA to Cellulose and Its DerivativesReferences; 3 Cellulose Activation and Dissolution; 3.1 Activation of Cellulose; 3.1.1 Introduction; 3.1.2 Accessibility and Its Methods of Determination; 3.1.3 Activation by Intercrystalline Swelling; 3.1.4 Activation by Intracrystalline Swelling; 3.2 Dissolution of Cellulose; 3.2.1 Non-derivatizing Solvents; 3.2.2 Derivatizing Solvents; References; 4 Principles of Cellulose Derivatization; 4.1 The Heterogeneous Versus the Homogeneous Reaction Path: Advantages and Limitations. | |
| 505 | 8 | |a 4.2 Esterification of Celluloseâ#x80;#x94;General Comments4.3 Etherification of Celluloseâ#x80;#x94;Overview; 4.4 Regioselective Synthesis of Cellulose Derivatives Using Protecting Groups; 4.4.1 Triphenylmethyl Ethers; 4.4.2 Trialkylsilyl Ethers; 4.4.3 3-O-Ethers of Cellulose; 4.4.4 Thermal Properties in Aqueous Solution; 4.4.5 Application of Orthogonal Protecting Groups; References; 5 Cellulose Esters; 5.1 Esters of Carboxylic Acids; 5.1.1 Industrial Preparation of Cellulose Esters; 5.1.2 Laboratory Synthesis of Cellulose Carboxylic Esters; 5.1.2.1 Heterogeneous Procedures. | |
| 520 | |a This book summarizes recent progress in cellulose chemistry. The last 10 years have witnessed important developments, because sustainability is a major concern. Biodegradable cellulose derivatives, in particular esters and ethers, are employed on a large scale. The recent developments in cellulose chemistry include unconventional methods for the synthesis of derivatives, introduction of novel solvents, e.g. ionic liquids, novel approaches to regioselective derivatization of cellulose, preparation of nano-particles and nano-composites for specific applications. These new developments are discussed comprehensively. This book is aimed at researchers and professionals working on cellulose and its derivatives. It fills an important gap in teaching, because most organic chemistry textbooks concentrate on the relatively simple chemistry of mono- and disaccharides. The chemistry and, more importantly, the applications of cellulose are only concisely mentioned. | ||
| 588 | 0 | |a Online resource; title from PDF title page (Ebsco, viewed February 19, 2018) | |
| 650 | 0 | |a Cellulose. |0 http://id.loc.gov/authorities/subjects/sh85021705. | |
| 650 | 0 | |a Cellulose |x Biotechnology. |0 http://id.loc.gov/authorities/subjects/sh2010002675. | |
| 650 | 0 | |a Cellulose |x Biodegradation. |0 http://id.loc.gov/authorities/subjects/sh85021706. | |
| 650 | 7 | |a Cellulose. |2 fast |0 (OCoLC)fst00850336. | |
| 650 | 7 | |a Cellulose |x Biodegradation. |2 fast |0 (OCoLC)fst00850338. | |
| 650 | 7 | |a Cellulose |x Biotechnology. |2 fast |0 (OCoLC)fst00850340. | |
| 700 | 1 | |a El Seoud, Omar A. |q (Omar Abdel), |e author. |0 http://id.loc.gov/authorities/names/no2001020593. | |
| 700 | 1 | |a Koschella, Andreas, |e author. |0 http://id.loc.gov/authorities/names/n2006078665 |1 http://isni.org/isni/0000000109591730. | |
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