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|a E 1.99:1772914
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|a E 1.99:1772914
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|a Dynamic reaction-induced phase separation in tunable, adaptive covalent networks
|h [electronic resource]
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|a Argonne, Ill. :
|b Argonne National Laboratory ;
|a Oak Ridge, Tenn. :
|b Distributed by the Office of Scientific and Technical Information, U.S. Department of Energy,
|c 2020.
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| 300 |
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|a Size: p. 5028-5036 :
|b digital, PDF file.
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|a text
|b txt
|2 rdacontent.
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|a computer
|b c
|2 rdamedia.
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|a online resource
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|a Published through Scitech Connect.
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|a 05/01/2020.
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|a "Journal ID: ISSN 2041-6520."
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|a "Other: 163321."
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|a ": US2208822."
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|a Herbert, Katie M. ; Getty, Patrick T. ; Dolinski, Neil D. ; Hertzog, Jerald E. ; de Jong, Derek ; Lettow, James H. ; Romulus, Joy ; Onorato, Jonathan W. ; Foster, Elizabeth M. ; Rowan, Stuart J. ; et al.
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|a USDOE.
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|a National Institute of Standards and Technology (NIST)
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|a A series of catalyst-free, room temperature dynamic bonds derived from a reversible thia-Michael reaction are utilized to access mechanically robust dynamic covalent network films. The equilibrium of the thiol addition to benzalcyanoacetate-based Michael-acceptors can be directly tuned by controlling the electron-donating/withdrawing nature of the Michael-acceptor. By modulating the composition of different Michael-acceptors in a dynamic covalent network, a wide range of mechanical properties and thermal responses can be realized. Additionally, the reported systems phase-separate in a process, coined dynamic reaction-induced phase separation (DRIPS), that yields reconfigurable phase morphologies and reprogrammable shape-memory behaviour as highlighted by the heat-induced folding of a predetermined structure.
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|b AC02-06CH11357.
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|b 1609076.
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|b 60NANB15D077.
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|b DMR-1420709.
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|a 37 inorganic, organic, physical, and analytical chemistry
|2 local.
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|a Inorganic, organic, physical, and analytical chemistry
|2 local.
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|a Argonne National Laboratory.
|4 res.
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|a National Science Foundation (U.S.).
|4 spn.
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|a United States.
|b Department of Energy.
|b Office of Scientific and Technical Information
|4 dst.
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|u https://www.osti.gov/servlets/purl/1772914
|z Full Text (via OSTI)
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|a .b128296343
|b 12-08-22
|c 12-08-22
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|p Can circulate
|a University of Colorado Boulder
|b Online
|c Online
|d Online
|e E 1.99:1772914
|h Superintendent of Documents classification
|i web
|n 1
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