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035 |a (TOE)6267595 
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086 0 |a E 1.99: conf-9109287--4 
086 0 |a E 1.99:lbl-31312 
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088 |a conf-9109287--4 
088 |a lbl-31312 
245 0 0 |a Tritiation methods and tritium NMR spectroscopy  |h [electronic resource] 
260 |a Washington, D.C. :  |b United States. Department of Energy ;  |a Oak Ridge, Tenn. :  |b distributed by the Office of Scientific and Technical Information, U.S. Department of Energy,  |c 1991. 
300 |a Pages: (6 p) :  |b digital, PDF file. 
336 |a text  |b txt  |2 rdacontent. 
337 |a computer  |b c  |2 rdamedia. 
338 |a online resource  |b cr  |2 rdacarrier. 
500 |a Published through SciTech Connect. 
500 |a 09/01/1991. 
500 |a "lbl-31312" 
500 |a " conf-9109287--4" 
500 |a "DE92004307" 
500 |a ": P41 RR01237" 
500 |a 4. international symposium on the synthesis and applications of isotopes and isotopically labeled compounds, Toronto (Canada), 3 Sep 1991. 
500 |a Jaiswal, D.K.; Morimoto, H.; Williams, P.G.; Salijoughian, M. 
520 3 |a We have used a simple process for the production of highly tritiated water and characterized the product species by ¹H and ³H NMR spectroscopy. The water is readily manipulated and used in subsequent reactions either as T₂O, CH₃COOT or CF₃COOT. Development of tritiated diimide has progressed to the point where cis-hydrogenated products at 1-20 Ci/mmole S.A. are possible. Tri-n-butyl tin tritide has been produced at >95% tritium content and well characterized by multinuclear NMR techniques. 27 refs., 3 figs. 
536 |b AC03-76SF00098. 
650 7 |a Imides.  |2 local. 
650 7 |a Labelling.  |2 local. 
650 7 |a Tin Hydrides.  |2 local. 
650 7 |a Water.  |2 local. 
650 7 |a Nmr Spectra.  |2 local. 
650 7 |a Organometallic Compounds.  |2 local. 
650 7 |a Tritium.  |2 local. 
650 7 |a Beta Decay Radioisotopes.  |2 local. 
650 7 |a Hydrides.  |2 local. 
650 7 |a Hydrogen Compounds.  |2 local. 
650 7 |a Hydrogen Isotopes.  |2 local. 
650 7 |a Isotopes.  |2 local. 
650 7 |a Light Nuclei.  |2 local. 
650 7 |a Nuclei.  |2 local. 
650 7 |a Organic Compounds.  |2 local. 
650 7 |a Beta-Minus Decay Radioisotopes.  |2 local. 
650 7 |a Organic Nitrogen Compounds.  |2 local. 
650 7 |a Oxygen Compounds.  |2 local. 
650 7 |a Radioisotopes.  |2 local. 
650 7 |a Spectra.  |2 local. 
650 7 |a Odd-Even Nuclei.  |2 local. 
650 7 |a Tin Compounds.  |2 local. 
650 7 |a Years Living Radioisotopes.  |2 local. 
650 7 |a Inorganic, Organic, Physical And Analytical Chemistry.  |2 edbsc. 
710 2 |a Lawrence Berkeley National Laboratory.  |4 res. 
710 1 |a United States.  |b Department of Energy.  |4 spn. 
710 1 |a United States.  |b Department of Health and Human Services.  |4 spn. 
710 1 |a United States.  |b Department of Energy.  |b Office of Scientific and Technical Information.  |4 dst. 
856 4 0 |u http://www.osti.gov/servlets/purl/6267595/  |z Online Access 
907 |a .b59821425  |b 03-06-23  |c 05-26-10 
998 |a web  |b 05-26-10  |c f  |d m   |e p  |f eng  |g    |h 0  |i 2 
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952 f f |p Can circulate  |a University of Colorado Boulder  |b Online  |c Online  |d Online  |e E 1.99: conf-9109287--4  |h Superintendent of Documents classification  |i web  |n 1